Model 1470E Eight Channel Potentiostat/Galvanostat
The mode 1470E is an eight channel
potentiostat/galvanostat. Each independent channel within the
1470E is controlled by its own dedicated high performance digital
signal processor, which provides accurate and instantaneous test
control, data averaging and safety limit functions. A wide range of
potentiostatic (voltage controlled) and galvanostatic (current
controlled) techniques may be performed, including:
- open circuit
- cyclic voltammetry
- constant level and scanned voltage / current controlled
techniques
- fast voltage / current pulse techniques (e.g. for mobile phone
cell tests)
- voltage / current step techniques
- linear polarization resistance techniques
- ohmic-drop measurements (for accurate equivalent series
resistance ESR analysis)
High-speed data acquisition
The 1470E is able to acquire DC data at 10,000 samples per
second, which allows the unit to make very accurate measurements of
the equivalent series resistance (ESR) of batteries, fuel cells and
supercapacitors using DC ohmic drop techniques. If required, the
10,000 samples per second data acquisition rate can be used in
extremely short bursts of 1 millisecond, for example immediately
after the cell current is reversed or interrupted in order to
measure the ESR. The 1470E can operate at different measurement
sample rates at each step in the experiment so high-speed data is
only acquired precisely where it is needed and the PC disk is not
filled with repetitive data.
The 1470E also provides data reduction and averaging techniques
to minimize noise on the data and to reduce PC data storage
requirements.
Safety / step termination limit checking
The high-speed digital signal processor on each channel of the
1470E reacts immediately when safety or step termination limits are
reached on the cell (the PC is not involved in this process) with
the obvious benefit of protecting test cells from being over-tested
or damaged.
The user is informed of safety limit trips, allowing appropriate
action to be taken where necessary.
Anode / cathode investigations
The 1470E has optional auxiliary voltage inputs that allow
monitoring of individual anode / cathode electrodes in a cell, or of
individual cells in a battery or fuel cell stack. The auxiliary
voltage DC measurements are synchronized with those from the main
channels, allowing detailed analysis of fast pulse or cyclic
voltammetry tests at multiple points within a stack.
High power DC tests
The 1470E provides 10V, ±4A stimulus to cells, but for tests on
higher power devices (larger batteries or fuel cell stacks) it may
be necessary to increase this range of operation. Higher current
tests can be performed by connecting a number of 1470E channels
together in parallel (since each channel has independently floating
electrodes), providing 8A, 12A, and even up to 32A stimulus to the
cell. If increased voltage range is also required, Solartron offer a
range of power boosters that are
able to boost the voltage and current level that is applied to the
cell.
Sequential Impedance Measurements
The 1470E includes the ability to be connected to a single model
1255B or 1252A
FRA, allowing AC impedance measurements to be made sequentially on
each active channel. DC conditions on each cell are maintained while
the FRA is switched between cells. This multiplexed measurement
method offers a cost effective solution when studying phenomena that
are changing slowing with respect to the time needed to make the
measurement.
Parallel Impedance Measurements
The 1470E can be used with one or more model
1455A/1451A Frequency Response Analyzers to allow AC impedance
measurements to be made. These FRAs offer a full range of
measurement methods, including single sine, multi-sine and FFT.
Because the FRAs are so closely integrated into the system it
is possible to switch instantaneously from DC tests such as cyclic
voltammetry to impedance analysis. There are no delays waiting for
FRAs to become available, as occurs in multichannel systems using a
single FRA connected via a a multiplexer, since each channel can
have its own FRA.
Model 14703A Temperature Measurement Option
When fitted with a 14703A temperature measurement option, the
1470E can measure 8 temperature inputs, one per channels, by
directly connecting to thermocouples of types E, J, K or T. The
option provides:
- Temperature safety limits
- Temperature measurement with plots vs. time
- Temperature step termination limits
and includes a thermocouple interface unit for cold junction
compensation, with a 1 meter connection cable to the 1470E.
Thermocouples must be chosen to suit temperature range requirements
and are therefore not included with this option.
Model 14702A Auxiliary Voltage Channels (similar to RE1, RE2)
Option
This option provides eight additional auxiliary voltage
measurement channels
Specifications
| Number of Channels |
8 independent
floating channels per unit |
| Counter Electrode |
|
Output voltage |
>+10 V,
-3 V w.r.t. LO |
|
Output current |
4 A, subject to
thermal protection limits |
|
Selectable bandwidth |
10 Hz,
100 Hz, 1 kHz, 10 kHz, 100 kHz,
1 MHz |
| Voltage
measurement inputs (RE1, RE2) |
|
Connections |
Driven shields for
wide bandwidth |
|
Maximum voltage |
+10 V /
-3 V |
|
Voltage ranges |
Auto-range or
manually selected 10 V, 1 V, 100 mV |
|
Accuracy |
±0.1% of range |
|
Voltage resolution |
3 µV |
|
ADC |
16 bit 10,000 samples
/ sec |
| Current
measurement input (WE) |
|
Maximum current per channel |
±4 A |
|
Current ranges |
Auto-range or manually selected
5 A, 500 mA, 50 mA, 5 mA, 500 µA,
50 µA |
|
Accuracy |
±0.1% of range |
|
Current resolution |
1.5 nA |
|
ADC |
16 bit 10,000 samples / sec |
| Experiment |
|
Maximum steps /
experiment |
100 |
|
Step types: |
|
|
voltage,
current |
constant, ramp, pulse
(includes high speed GSM), cyclic voltammetry |
|
power,
resistance |
constant level
(discharge only) |
|
other |
rest (open circuit),
loop |
|
impedance |
requires one or more
frequency response analyzers |
|
Step termination
limits |
voltage, current,
power, resistance and charge.
temperature (requires option 14703A) |
|
Time to switch test
type |
100 µsec |
|
Minimum sample rate |
1 sample / 100
seconds |
|
Maximum sample rate |
10,000 samples /
second |
|
Measurement modes |
Fixed sample rate or
measure on change |
|
Shutdown safety
limits |
voltage, current
temperature (requires option 14703A) |
|
Temperature control |
Eurotherm 2000 Series
controllers |
| Temperature Range |
|
Operating |
5° to 40°C (41° to
104°F) |
|
Specified accuracy |
10° to 30°C |
|
Storage |
-25° to 70°C (-13°
to 158°F) |
| Interface |
|
|
Ethernet 10BaseT or
IEEE488 (GPIB) |
For instrument
control |
| Power Requirements |
|
|
Voltage |
90 to 264VAC |
|
Frequency |
47 to 63 Hz |
|
Power |
<
1000 VA |
| Dimensions |
|
|
Width |
450 mm
(17.7") |
|
Depth |
496 mm (19.5
") |
|
Height |
286 mm
(11.3") |
| Weight |
18 kg
(40 lbs) |
|
|
|
| 14703A Option
Specification - Temperature Measurement & Control
Outputs |
|
Temperature
measurement |
|
|
Temperature inputs |
8 (one
per main channel) |
|
Thermocouple types |
E, J, K,
T |
|
Temperature accuracy |
±1°C
(plus thermocouple errors) |
|
|
Min
(°C) |
Max
(°C) |
Resolution (°C) |
|
Type E |
-200 |
1000 |
0.0625 |
|
Type J |
-210 |
1200 |
0.0625 |
|
Type K |
-200 |
1372 |
0.0625 |
|
Type T |
-200 |
400 |
0.0625 |
|
|
|
|
|
|
The
14703A option provides:
- Temperature safety limits
- Temperature measurement with plots vs time
- Temperature step termination limits
Thermocouple Interface Unit included - for cold junction
compensation (with 1 metre connection cable to 1470).
Thermocouples must be chosen to suit temperature range
requirements and are therefore not supplied with this
option. |
|
Control
Outputs |
|
Number |
24 (three per main
channel) |
|
Switch type |
Opto-isolated
solid-state switches (similar to relays) |
|
Connections |
2 per switch |
|
Maximum voltage |
50 V |
|
Maximum current |
100 mA |
|
Control outputs can
be automatically switched on / off at each step in the
experiment to control external devices (relays, lamps,
heaters, gas valves, power boosters etc.).
Supplied with a D-type connector for customers to make up
their own connection leads.
|
| 14702A Option
Specification - Auxiliary Voltage Channels (similar to RE1,
RE2) |
|
Connections |
Driven shields for
wide bandwidth |
|
Maximum voltage |
+10 V /
-3 V |
|
Voltage ranges |
Auto-range,
10 V, 1 V, 100 mV |
|
Accuracy |
±0.1% of range |
|
Voltage resolution |
3 μV |
|
ADC |
16 bit 10,000 samples
/ sec |
|
Input impedance |
>10 GΩ |
|
DC measurements |
synchronized to
assigned main channel |
|
Cell connection cable
set for 14702A |
8 channel cable set
included (1 metre length) |
|
IMPORTANT NOTE:
Option 14702A requires 14703A to be fitted. |
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