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Model 1470E Eight Channel Potentiostat/Galvanostat

Model 1470E Eight Channel Potentiostat/Galvanostat

The mode 1470E is an eight channel potentiostat/galvanostat.  Each independent channel within the 1470E is controlled by its own dedicated high performance digital signal processor, which provides accurate and instantaneous test control, data averaging and safety limit functions. A wide range of potentiostatic (voltage controlled) and galvanostatic (current controlled) techniques may be performed, including:

  • open circuit
  • cyclic voltammetry
  • constant level and scanned voltage / current controlled techniques
  • fast voltage / current pulse techniques (e.g. for mobile phone cell tests)
  • voltage / current step techniques
  • linear polarization resistance techniques
  • ohmic-drop measurements (for accurate equivalent series resistance ESR analysis)

High-speed data acquisition
The 1470E is able to acquire DC data at 10,000 samples per second, which allows the unit to make very accurate measurements of the equivalent series resistance (ESR) of batteries, fuel cells and supercapacitors using DC ohmic drop techniques. If required, the 10,000 samples per second data acquisition rate can be used in extremely short bursts of 1 millisecond, for example immediately after the cell current is reversed or interrupted in order to measure the ESR. The 1470E can operate at different measurement sample rates at each step in the experiment so high-speed data is only acquired precisely where it is needed and the PC disk is not filled with repetitive data.

The 1470E also provides data reduction and averaging techniques to minimize noise on the data and to reduce PC data storage requirements.

Safety / step termination limit checking
The high-speed digital signal processor on each channel of the 1470E reacts immediately when safety or step termination limits are reached on the cell (the PC is not involved in this process) with the obvious benefit of protecting test cells from being over-tested or damaged.

The user is informed of safety limit trips, allowing appropriate action to be taken where necessary.

Anode / cathode investigations
The 1470E has optional auxiliary voltage inputs that allow monitoring of individual anode / cathode electrodes in a cell, or of individual cells in a battery or fuel cell stack. The auxiliary voltage DC measurements are synchronized with those from the main channels, allowing detailed analysis of fast pulse or cyclic voltammetry tests at multiple points within a stack.

High power DC tests
The 1470E provides 10V, ±4A stimulus to cells, but for tests on higher power devices (larger batteries or fuel cell stacks) it may be necessary to increase this range of operation. Higher current tests can be performed by connecting a number of 1470E channels together in parallel (since each channel has independently floating electrodes), providing 8A, 12A, and even up to 32A stimulus to the cell. If increased voltage range is also required, Solartron offer a range of power boosters that are able to boost the voltage and current level that is applied to the cell.

Sequential Impedance Measurements
The 1470E includes the ability to be connected to a single model 1255B or 1252A FRA, allowing AC impedance measurements to be made sequentially on each active channel. DC conditions on each cell are maintained while the FRA is switched between cells. This multiplexed measurement method offers a cost effective solution when studying phenomena that are changing slowing with respect to the time needed to make the measurement.

Parallel Impedance Measurements
The 1470E can be used with one or more model 1455A/1451A Frequency Response Analyzers to allow AC impedance measurements to be made. These FRAs offer a full range of measurement methods, including single sine, multi-sine and FFT. Because the  FRAs are so closely integrated into the system it is possible to switch instantaneously from DC tests such as cyclic voltammetry to impedance analysis. There are no delays waiting for FRAs to become available, as occurs in multichannel systems using a single FRA connected via a a multiplexer, since each channel can have its own FRA.

Model 14703A Temperature Measurement Option
When fitted with a 14703A temperature measurement option, the 1470E can measure 8 temperature inputs, one per channels, by directly connecting to thermocouples of types E, J, K or T. The option provides:

  • Temperature safety limits
  • Temperature measurement with plots vs. time
  • Temperature step termination limits

and includes a thermocouple interface unit for cold junction compensation, with a 1 meter connection cable to the 1470E. Thermocouples must be chosen to suit temperature range requirements and are therefore not included with this option.

Model 14702A Auxiliary Voltage Channels (similar to RE1, RE2) Option
This option provides eight additional auxiliary voltage measurement channels

 

Specifications

Number of Channels 8 independent floating channels per unit
Counter Electrode
Output voltage >+10 V, -3 V w.r.t. LO
Output current 4 A, subject to thermal protection limits
Selectable bandwidth 10 Hz, 100 Hz, 1 kHz, 10 kHz, 100 kHz, 1 MHz
Voltage measurement inputs (RE1, RE2)
Connections Driven shields for wide bandwidth
Maximum voltage +10 V / -3 V
Voltage ranges Auto-range or manually selected 10 V, 1 V, 100 mV
Accuracy ±0.1% of range
Voltage resolution 3 µV
ADC 16 bit 10,000 samples / sec
Current measurement input (WE)
Maximum current per channel ±4 A
Current ranges Auto-range or manually selected 5 A, 500 mA, 50 mA, 5 mA, 500 µA, 50 µA
Accuracy ±0.1% of range
Current resolution 1.5 nA
ADC 16 bit 10,000 samples / sec
Experiment
Maximum steps / experiment 100
Step types:
  voltage, current constant, ramp, pulse (includes high speed GSM), cyclic voltammetry
  power, resistance constant level (discharge only)
  other rest (open circuit), loop
  impedance  requires one or more frequency response analyzers
Step termination limits voltage, current, power, resistance and charge. 
temperature (requires option 14703A)
Time to switch test type 100 µsec
Minimum sample rate 1 sample / 100 seconds
Maximum sample rate 10,000 samples / second
Measurement modes Fixed sample rate or measure on change
Shutdown safety limits voltage, current
temperature (requires option 14703A)
Temperature control Eurotherm 2000 Series controllers
Temperature Range
Operating 5° to 40°C (41° to 104°F)
Specified accuracy 10° to 30°C
Storage -25° to 70°C (-13° to 158°F)
Interface
Ethernet 10BaseT or IEEE488 (GPIB) For instrument control
Power Requirements
Voltage 90 to 264VAC
Frequency 47 to 63 Hz
Power <  1000 VA 
Dimensions
Width 450 mm (17.7")
Depth 496  mm (19.5 ")
Height 286 mm (11.3")
Weight 18 kg (40 lbs)
14703A Option Specification - Temperature Measurement & Control Outputs
Temperature measurement
Temperature inputs 8 (one per main channel)
Thermocouple types E, J, K, T
Temperature accuracy ±1°C (plus thermocouple errors)
Min (°C) Max (°C) Resolution (°C)
Type E -200 1000 0.0625
Type J -210 1200 0.0625
Type K -200 1372 0.0625
Type T -200 400 0.0625
The 14703A option provides:
  • Temperature safety limits
  • Temperature measurement with plots vs time
  • Temperature step termination limits

Thermocouple Interface Unit included - for cold junction compensation (with 1 metre connection cable to 1470).

Thermocouples must be chosen to suit temperature range requirements and are therefore not supplied with this option.

Control Outputs
Number 24 (three per main channel)
Switch type Opto-isolated solid-state switches (similar to relays)
Connections 2 per switch
Maximum voltage 50 V
Maximum current 100 mA
Control outputs can be automatically switched on / off at each step in the experiment to control external devices (relays, lamps, heaters, gas valves, power boosters etc.).

Supplied with a D-type connector for customers to make up their own connection leads.

 

14702A Option Specification - Auxiliary Voltage Channels (similar to RE1, RE2)
Connections Driven shields for wide bandwidth
Maximum voltage +10 V / -3 V
Voltage ranges Auto-range, 10 V, 1 V, 100 mV
Accuracy ±0.1% of range
Voltage resolution 3 μV
ADC 16 bit 10,000 samples / sec
Input impedance >10 GΩ
DC measurements synchronized to assigned main channel
Cell connection cable set for 14702A 8 channel cable set included (1 metre length)
IMPORTANT NOTE: Option 14702A requires 14703A to be fitted.

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